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Pyrolysis of biomass into biochar and application of a carbon-rich product to water and soil media have been demonstrated to be effective in sequestering of contaminants. Fundamentally, biochar characteristics are controlled by feedstock and pyrolysis variables. The present study investigated the effects of synthesis variables (highest treatment temperature, heating rate and residence time) on biochar sorption properties. Oil palm empty fruit bunch (EFB) and rice husk (RH) biomasses were compared as initial feedstock. The variables were optimized using response surface methodology (RSM) to optimize the values of responses including biochars organic carbon content, cation exchange capacity (CEC), surface area and pores volume. Sorption performances of the optimized biochars were further investigated in removal of a polar imidazolinone herbicide from soil. Based on the results, pyrolysis temperature was …