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In this paper, the results of a laboratory investigation conducted with heat evolution of high-volume fly ash (HVFA) concrete are presented. Heat evolution of concrete was studied by measuring the temperature increase in concrete under adiabatic curing condition. Characteristic of heat evolution of fly ash concrete was found to be strongly dependent on the replacement level of fly ash and dosage of superplasticizer used to maintain workability. It was also found that using fly ash as cement replacement resulted in a reduction on the maximum temperature rise. Increasing the replacement level of fly ash caused lower temperature rise in concrete. Superplasticizer caused a delay in peak temperature rise time; this is taken as an indicator that high-dosage superplasticizer used in concrete caused retardation in hydration of cement. Concretes having similar ingredients showed similar peak temperature rise whether they …