Authors
Carlo Bicchi, Claudio Brunelli, Chiara Cordero, Patrizia Rubiolo, Mario Galli, Albino Sironi
Publication date
2004/1/23
Journal
Journal of Chromatography A
Volume
1024
Issue
1-2
Pages
195-207
Publisher
Elsevier
Description
This study applies Ultrafast module-GC (UFM-GC) with direct resistively heated columns to routine analysis of a group of essential oils of differing complexities (chamomile, peppermint, rosemary and sage). Essential oils were analysed by conventional GC with conventional inner diameter (i.d.) columns (0.25mm) of different lengths (5 and 25m long) and by Fast GC and Ultrafast module-GC with narrow bore columns (0.1mm i.d., 5m long). Column performance were evaluated and compared through their Grob test, separation number and peak capacity. Ultrafast module-GC was successful in the qualitative and quantitative analysis of essential oils of different compositions with analysis times between 40s and 2min versus 20–60min required by conventional GC. Critical pairs or groups of components were separated by carefully tuning selectivity of the stationary phase to compensate for loss of efficiency due to the …
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